Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl Acrylate → Ethyl 3-[4-(4-chlorobenzyl)-piperazin-1-yl]-propionate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl Acrylate | HCID 8821 | — |
| 반응물 | 4-Chlorobenzylpiperazine | HCID 134826 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Ethyl 3-[4-(4-chlorobenzyl)-piperazin-1-yl]-propionate | HCID 20326894 | 92.8% |
반응 단계
Analogously to Example 1a, 30 g (0.3 mol) ethyl acrylate and 63.2 g 1-(4-chlorobenzyl)-piperazine are reacted in 200 ml ethanol to give 86.5 g (92.8% of theory) ethyl 3-[4-(4-chlorobenzyl)-piperazin-1-yl]-propionate; b.p. 150° - 160° C./0.1 mm Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04092416 |
| 출처 데이터셋 | uspto-grants-1978_05 |
| ORD ID | ord-323212d42a5a467087745b51dab23c98 |
| 출처 메모 | uspto-grants-1978_05 |