Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Chloride → N,N-Dimethyl-N-(2-benzoylaminoethyl)benzylammonium Chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Chloride | HCID 7503 | — |
| 반응물 | N-(2-(Dimethylamino)ethyl)benzamide | HCID 113158 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N,N-Dimethyl-N-(2-benzoylaminoethyl)benzylammonium Chloride | HCID 19811098 | — |
반응 단계
A solution of 19.23 grams (0.10 mol) of the N-(2-dimethylaminoethyl)benzamide, prepared as described in Example 1, 12.66 grams (0.10 mol) of α-chlorotoluene and 64 milliters of acetonitrile was heated at reflux for 19.75 hours. Solid crystallized on cooling which was collected, washed with acetonitrile and dried. The yield of product was 24.0 grams (75.27% of theory); mp=175°-176° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05162188 |
| 출처 데이터셋 | uspto-grants-1992_11 |
| ORD ID | ord-80630acfb6e64d19be126317e4c1d130 |
| 출처 메모 | uspto-grants-1992_11 |