Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Dodecanamide, N-[2-[(2-hydroxyethyl)amino]ethyl]-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Chloride | HCID 5234 | — |
| 반응물 | 1-(2-Hydroxyethyl)-2-undecylimidazoline | HCID 8709 | — |
| 생성물 | Dodecanamide, N-[2-[(2-hydroxyethyl)amino]ethyl]- | HCID 66937 | — |
반응 단계
22 g of 1-(2-hydroxyethyl)-2-undecyl-2-imidazoline and 300 ml of water was stirred at 40°-50° C. for 24 hours. The resulting soapy solution was salted with 50 g of NaCl and then extracted with 500 ml ethyl acetate. The organic layer was dried, filtered and concentrated to give 23 g of solid. This material was dissolved in hexane by heating at 50 C. for 2 hrs., then cooled to room temperature and filtered to afford 18.8 g of pure product, m.p. 92°-94° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05162315 |
| 출처 데이터셋 | uspto-grants-1992_11 |
| ORD ID | ord-60870d4e1b7d4476988222558a05d4da |
| 출처 메모 | uspto-grants-1992_11 |