Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloroaniline → 1-(4-Trifluoromethylbenzoyl)-3-(4-chlorophenyl)urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloroaniline | HCID 7812 | — |
| 반응물 | 4-Trifluoromethylbenzoylisocyanate | HCID 14913744 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 1-(4-Trifluoromethylbenzoyl)-3-(4-chlorophenyl)urea | HCID 19808581 | — |
반응 단계
To a stirred solution of 1.08 g of 4-trifluoromethylbenzoylisocyanate in 5 ml of dry diethylether is added a solution of 0.64 g of 4-chloroaniline in 50 ml of acetonitrile. A precipitate is immediately formed. The precipitate is sucked off and washed with acetonitrile. The title compound is obtained a yield of 1.1 g; melting point 260° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05166180 |
| 출처 데이터셋 | uspto-grants-1992_11 |
| ORD ID | ord-635c071f4e224bc496b5380db9ca225c |
| 출처 메모 | uspto-grants-1992_11 |