Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → 4-(4-(2-Quinolinylmethylsulfonyl)styryl)benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Hydrogen Peroxide | HCID 784 | — |
| 반응물 | 4-(4-(2-Quinolinylmethylsulfinyl)styryl)benzoic acid | HCID 54512756 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-(4-(2-Quinolinylmethylsulfonyl)styryl)benzoic acid | HCID 54457133 | — |
반응 단계
To 3 mmol of the sulfinyl compound from Step A in acetic acid (40 mmol) is added 30% hydrogen peroxide (2 ml). The mixture is stirred at ambient temperature and assayed by TLC. Upon disappearance of the sulfinyl starting compound, the reaction mixture is diluted with dichloromethane, washed with dilute aqueous sodium bisulfite and water, dried and evaporated to give 4-(4-(2-quinolinylmethylsulfonyl)styryl)benzoic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05166210 |
| 출처 데이터셋 | uspto-grants-1992_11 |
| ORD ID | ord-01cf7ebcee884278be3216537458d942 |
| 출처 메모 | uspto-grants-1992_11 |