N-methyl-2-pyrrolidone → S-octadecyl thiocarbamate

HRID 374621노트

반응식

HRID 374621 반응식
[CH2:1]([SH:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].C[N:21]1CCC[C:22]1=[O:26]>>[C:22](=[O:26])([S:19][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[NH2:21]

참가 물질

3

반응물 2

HCID 13387N-methyl-2-pyrrolidoneHCID 179051-Octadecanethiol

생성물 1

HCID 18997609S-octadecyl thiocarbamate수율 60%

실험 절차

As described in Example 17, but using 63 g of 1-octadecylmercaptan (0.22 mol) dissolved in 30 ml of N-methylpyrrolidone, S-octadecyl thiocarbamate was obtained in a yield of 60% of theory.

출처 및 근거

ORD 기록
ord-619c694ec8eb44a38260df4d86112468
출처 데이터셋
uspto-grants-1996_01
특허 번호
US05481035

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