Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoroacetic acid → Caprine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoroacetic acid | HCID 6422 | — |
| 반응물 | tert-butyl (2S)-2-aminohexanoate | HCID 12451446 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Caprine | HCID 21236 | — |
반응 단계
23.5 mg of L-N-[(2R or S)-5-ethylthio-2-(1-naphthylmethyl)pentanoyl]norleucine tert-butyl ester was dissolved in 0.2 ml of dichloromethane, and 0.1 ml of trifluoro acetic acid was added thereto. The mixture was stirred at room temperature for four hours. Then, the reaction solution was concentrated under reduced pressure to obtain 20.7 mg of L-N-[(2R or S)-5-ethylthio-2-(1-naphthylmethyl)pentanoyl]norleucine as colorless solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05481036 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-aa312e5f1bd544c6952f2a6f19a3f20f |
| 출처 메모 | uspto-grants-1996_01 |