2-Ethoxybenzoyl chloride → 2-(2-Ethoxybenzamido)-3-methylbenzamide

반응식

[NH2:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5].[CH2:12]([O:14][C:15]1[CH:23]=[CH:22][CH:21]=[CH:20][C:16]=1[C:17](Cl)=[O:18])[CH3:13]>>[CH2:12]([O:14][C:15]1[CH:23]=[CH:22][CH:21]=[CH:20][C:16]=1[C:17]([NH:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5])=[O:18])[CH3:13]

참가 물질

반응물 2

HCID 30163972-Ethoxybenzoyl chloride

HCID 142218072-Amino-3-methylbenzamide

생성물 1

HCID 185365992-(2-Ethoxybenzamido)-3-methylbenzamide

실험 절차

The title compound was prepared from 2-amino-3-methylbenzamide (Chem. Pharm. Bull., 1988, 36, 2955) and 2-ethoxybenzoyl chloride following the procedure of Preparation 5 and was obtained as colorless crystals (71%), m.p. 197°-200° C. Found: C,68.80; H,5.99; N,9.36. C17H18N2O3 requires C,68.44; H,6.08; N,9.39%.

후처리

customthe procedure of Preparation 5

출처 및 근거

ORD 기록: ord-b2fd3165b0224357bf996d9e9cdaaf9b
출처 데이터셋: uspto-grants-1996_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05482941

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