2-Amino-3-methylbenzamide → 3-Methyl-2-(2-n-propoxyphenyl)benzamide

반응식

N[C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5].[CH2:12]([O:15][C:16]1[CH:24]=[CH:23][CH:22]=[CH:21][C:17]=1C(Cl)=O)[CH2:13][CH3:14]>>[CH3:11][C:10]1[C:2]([C:17]2[CH:21]=[CH:22][CH:23]=[CH:24][C:16]=2[O:15][CH2:12][CH2:13][CH3:14])=[C:3]([CH:7]=[CH:8][CH:9]=1)[C:4]([NH2:6])=[O:5]

참가 물질

반응물 2

HCID 142218072-Amino-3-methylbenzamide

HCID 159219132-Propoxybenzoyl chloride

생성물 1

HCID 189957873-Methyl-2-(2-n-propoxyphenyl)benzamide

실험 절차

The title compound was prepared from 2-amino-3-methylbenzamide and 2-n-propoxybenzoyl chloride following the procedure of Preparation 5 and was obtained as a colorless solid (71%), m.p. 140°-142° C. Found: C,69.39; H,6.58; N,8.98. C18H20N2O3 requires C,69.21; H,6.45; N,8.97%.

후처리

customthe procedure of Preparation 5

출처 및 근거

ORD 기록: ord-c34332d179c54d928a2c3861f8e773f6
출처 데이터셋: uspto-grants-1996_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05482941

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