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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 374843생성일: 2026년 10월 26일

2,3-Dichloro-1,1,1,4,4,4-hexafluorobut-2-ene → 2-(1-Chloro-2,2,2-trifluoroethyl)-2-trifluoromethyl-[1,3]-dioxolo[4,5-b]pyridine

https://huagongshe.com/reaction/374843

반응식

참여 물질

역할이름HCID투입량
반응물2,3-Dichloro-1,1,1,4,4,4-hexafluorobut-2-eneHCID 9337—
반응물HCID 178516237HCID 178516237—
생성물2-(1-Chloro-2,2,2-trifluoroethyl)-2-trifluoromethyl-[1,3]-dioxolo[4,5-b]pyridineHCID 18995942—

반응 단계

11 g of 2,3-dihydroxypyridine were reacted with 23.5 g of 2,3-dichloro-1,1,1,4,4,4-hexafluoro-2-butene as described in Example 2. After distillation under a high vacuum, the product was obtained in the form of colourless crystals in an amount of 15.5 g (=50% of theory). The NMR spectra showed the following characteristic absorptions: 19F-NMR: -68.5 and -81.6 ppm. 1H-NMR 4.81 ppm.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05482956
출처 데이터셋uspto-grants-1996_01
ORD IDord-2fe2a5ad99d740f79b58f5cc8a2e6c32
출처 메모uspto-grants-1996_01