Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Ethylhexanal → 5-Amino-5-hydroxymethyl-2-(3-heptyl)-1,3-dioxane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Ethylhexanal | HCID 31241 | — |
| 반응물 | Tris(hydroxymethyl)nitromethane | HCID 31337 | — |
| 생성물 | 5-Amino-5-hydroxymethyl-2-(3-heptyl)-1,3-dioxane | HCID 18996049 | 95.1% |
반응 단계
Procedure of Example 2 was repeated with 6.41 g of 2-ethylhexanal and 7.56 g of 2-(hydroxymethyl)-2-nitro-1,3-propanediol to give 11 g of 5-nitro-5-hydroxymethyl-1,3-dioxane derivative, which was reduced and distilled at 175°-178° C. to give 8.7 g of the product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05482965 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-3a82a3418c454d79b570a00b1fb4f332 |
| 출처 메모 | uspto-grants-1996_01 |