Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Octylbenzene → HCID 13742410, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Octylbenzene | HCID 16607 | — |
| 반응물 | Glyoxal, phenyl-, hydrate | HCID 12215922 | — |
| 촉매 | Titanium Tetrachloride | HCID 24193 | — |
| 용매 | 1,1-Dichloroethane | HCID 6365 | — |
| 생성물 | HCID 13742410 | HCID 13742410 | — |
반응 단계
Phenylglyoxal monohydrate (608 mg, 4 mM) and n-octylbenzene (1.77 ml, 8 mM) were dissolved in dichloroethane (8 ml), titanium tetrachloride (0.66 ml, 6 mM) was added, and reacted at room temperature for 30 minutes. Using the same procedure as in Example 1, 4'-n-octylbenzoin was obtained as crystal (810.0 mg, 62.6% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05484689 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-7915a95a149c4f35a700216a2be8fa61 |
| 출처 메모 | uspto-grants-1996_01 |