Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethylamine → N-Ethyl-2-(4-nitro-1H-imidazol-1-yl)octanoamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethylamine | HCID 6341 | — |
| 반응물 | Ethyl 2-(4-nitro-1H-imidazole-1-yl)octanoate | HCID 10062368 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-Ethyl-2-(4-nitro-1H-imidazol-1-yl)octanoamide | HCID 15222339 | — |
반응 단계
Ethyl 2-(4-nitro-1H-imidazol-1-yl)octanoate (17 moles, 5.0 g) and ethylamine (20 ml) were stirred in 150 ml ethanol at room temperature for 16 hours. The reaction was added to ice water, extracted with ethyl acetate, washed with water, dried over sodium sulfate and concentrated. The oil crystallized upon standing to yield 3.9 g of N-Ethyl-2-(4-nitro-1H-imidazol-1-yl)octanoamide. (MS).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05484780 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-fd4c582d41ef494f8ba2e0064e6fd39f |
| 출처 메모 | uspto-grants-1996_01 |