3,4-Dimethoxycarbonyl-2-methoxy-6-methyl-5-nitropyridine → HCID 15289707, 화합물
반응식
[CH3:1][O:2][C:3]([C:5]1[C:6]([O:19][CH3:20])=[N:7][C:8]([CH3:18])=[C:9]([N+:15]([O-])=O)[C:10]=1[C:11]([O:13][CH3:14])=[O:12])=[O:4]>C(OCC)(=O)C.[Pd]>[NH2:15][C:9]1[C:8]([CH3:18])=[N:7][C:6]([O:19][CH3:20])=[C:5]([C:3]([O:2][CH3:1])=[O:4])[C:10]=1[C:11]([O:13][CH3:14])=[O:12]참가 물질
4
실험 절차
In 5 ml of ethyl acetate was dissolved 350 mg of 3,4-dimethoxycarbonyl-2-methoxy-6-methyl-5-nitropyridine, and 300 mg of 10% Pd-C (50% wet) was added to the solution. Catalytic reduction reaction was conducted for 4.5 hours. After the reaction mixture was dried over magnesium sulfate, the solvent was distilled off to afford an oily product.
후처리
- additionwas added to the solution
- customCatalytic reduction reaction
- dry with materialAfter the reaction mixture was dried over magnesium sulfate
- distillationthe solvent was distilled off
- customto afford an oily product
출처 및 근거
- ORD 기록
- ord-c41010b4ebab483b8d14b7720d002562
- 출처 데이터셋
- uspto-grants-1995_05
- 특허 번호
- US05420275
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