Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → N-(hydroxymethyl)acetamide acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Formicin | HCID 69365 | — |
| 촉매 | Pyridine | HCID 1049 | — |
| 생성물 | N-(hydroxymethyl)acetamide acetate | HCID 86745977 | 900% |
반응 단계
Acetic anhydride (25 g) and pyridine (10 drops) is added to N-(hydroxymethyl)acetamide (9 g, 0.1 mol). The reaction mixture is stirred overnight at room temperature, concentrated in vacuo and chased with xylene to give the title product as an oil (11.9 g, 0.9 mol) which is identified by 1HNMR spectral analysis.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05484807 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-452be2e369b949f39458cfbb65e5b732 |
| 출처 메모 | uspto-grants-1996_01 |