참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | 4-Fluoro-2-nitroaniline | HCID 67769 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Bromo-4-fluoro-6-nitroaniline | HCID 292004 | — |
반응 단계
Mix 4-fluoro-2-nitroaniline (15.6 g, 0.1 mol) in water (400 mL ) and add 48% hydrobromic acid (1 kg). Add bromine (16 g, 0.1 mol) with stirring and stir for 1 hour. Dilute to 2 L and cool to 7° C. Filter, wash with water and dry to give 4-fluoro-2-bromo-6-nitroaniline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05484814 |
|---|
| 출처 데이터셋 | uspto-grants-1996_01 |
|---|
| ORD ID | ord-333d92422a9143198fb78df251fa21b3 |
|---|
| 출처 메모 | uspto-grants-1996_01 |
|---|
