Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3-Dimethoxycinnamic acid → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,3-dimethoxyphenyl)ethenyl)-, (E)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3-Dimethoxycinnamic acid | HCID 99525 | — |
| 반응물 | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| 생성물 | 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,3-dimethoxyphenyl)ethenyl)-, (E)- | HCID 6448851 | 46% |
반응 단계
Substantially the same procedure as in Example 7 was repeated using 2.0 g (10.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.52 g (12.1 mmol) of 2,3dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylsulfoxide/water to give 1.72 g (yield 46%) of Compound 66 as a white powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05484920 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-3224eae34c3b4d24b02b739ea1630b29 |
| 출처 메모 | uspto-grants-1996_01 |