Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(1,3-Benzodioxol-5-yl)prop-2-enoic acid → 1H-Purine-2,6-dione, 8-((1E)-2-(1,3-benzodioxol-5-yl)ethenyl)-3,7-dihydro-1,3-dimethyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(1,3-Benzodioxol-5-yl)prop-2-enoic acid | HCID 16917 | — |
| 반응물 | 5,6-Diamino-1,3-dimethyluracil | HCID 79501 | — |
| 생성물 | 1H-Purine-2,6-dione, 8-((1E)-2-(1,3-benzodioxol-5-yl)ethenyl)-3,7-dihydro-1,3-dimethyl- | HCID 6062002 | 13% |
반응 단계
Substantially the same procedure as in Example 7 was repeated using 5.0 g (29.4 mmol) of 5,6-diamino-1,3 -dimethyluracil and 6.78 g (35.3 mmol) of 3,4-methylenedioxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/water to give 1.20 g (yield 13%) of Compound 86 as a pale yellow powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05484920 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-03f99e4dd4cd457489f3441c78c72507 |
| 출처 메모 | uspto-grants-1996_01 |