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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 375317생성일: 2026년 10월 24일

5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedione → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxy-3-methylphenyl)ethenyl)-1,3-dipropyl-, (E)-

https://huagongshe.com/ko/reaction/375317

반응식

참여 물질

역할이름HCID투입량
반응물5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedioneHCID 5098605—
반응물2,4-Dimethoxy-3-methylcinnamic acidHCID 53401577—
생성물1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxy-3-methylphenyl)ethenyl)-1,3-dipropyl-, (E)-HCID 644877850.1%

반응 단계

Substantially the same procedure as in Reference Example 1 was repeated using 1.25 g (5.52 mmol) of 5,6-diamino-1,3-dipropyluracil and 1.35 g (6.08 mmol) of 2,4 -dimethoxy-3-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 1.14 g (yield 50%) of Compound 14 as white needles.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05484920
출처 데이터셋uspto-grants-1996_01
ORD IDord-f37beccbaa9844cd9dbf844f1c99ffe1
출처 메모uspto-grants-1996_01