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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 375327생성일: 2026년 10월 24일

3-(2-Chlorophenyl)acrylic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2-chlorophenyl)ethenyl)-1,3-dipropyl-, (E)-

https://huagongshe.com/ko/reaction/375327

반응식

참여 물질

역할이름HCID투입량
반응물3-(2-Chlorophenyl)acrylic acidHCID 19567—
반응물5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedioneHCID 5098605—
생성물1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2-chlorophenyl)ethenyl)-1,3-dipropyl-, (E)-HCID 644878882%

반응 단계

Substantially the same procedure as in Reference Example 1 was repeated using 3.00 g (13.3 mmol) of 5,6-diamino-1,3-dipropyluracil and 2.67 g (14.6 mmol) of 2-chlorocinnamic acid. Then, the resultant crude crystals were recrystallized from toluene to give 3.72 g (yield 82%) of Compound 40 as white needles.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05484920
출처 데이터셋uspto-grants-1996_01
ORD IDord-8983c88acb5f4a9391fbf53c298cba1e
출처 메모uspto-grants-1996_01