Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2-Pyrrolidinophenyl)acetic acid hydrobromide → (4aRS,7aRS)6-{[2-(1-pyrrolidinyl)phenyl]acetyl}4,4-diphenylperhydrothiopyrano[2,3-c]pyrrole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2-Pyrrolidinophenyl)acetic acid hydrobromide | HCID 67745326 | — |
| 반응물 | (4aRS,7aRS)4,4-diphenylperhydrothiopyrano[2,3-c]pyrrole hydrochloride | HCID 67745331 | — |
| 생성물 | (4aRS,7aRS)6-{[2-(1-pyrrolidinyl)phenyl]acetyl}4,4-diphenylperhydrothiopyrano[2,3-c]pyrrole | HCID 67745328 | 30.9% |
반응 단계
By carrying out the procedure as in Example of Use 1, using 1.85 g of [2-(1-pyrrolidinyl)phenyl]acetic acid hydrobromide and 2.0 g of (4aRS,7aRS)4,4-diphenylperhydrothiopyrano[2,3-c]pyrrole hydrochloride, 0.90 g of (4aRS,7aRS)6-{[2-(1-pyrrolidinyl)phenyl]acetyl}4,4-diphenylperhydrothiopyrano[2,3-c]pyrrole is obtained in the form of white crystals; melting point 166° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05484942 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-f3f4f2325da44750b66b45e54d18e8bb |
| 출처 메모 | uspto-grants-1996_01 |