Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-(3-Fluorophenyl)propanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-(3-Fluorophenyl)propionic acid | HCID 2737489 | — |
| 생성물 | 3-(3-Fluorophenyl)propanoyl chloride | HCID 18993501 | — |
반응 단계
A solution of 3-fluorohydrocinnamic acid (28 g) in thionyl chloride (90 ml) was heated at reflux for 3 hours. 3-Fluorohydrocinnamoyl chloride (27 g) was isolated by distillation (150°-110° C. @ ca 20 mm.Hg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05486541 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-66e7a4465c454ece8d230e1ae0a91cbd |
| 출처 메모 | uspto-grants-1996_01 |