Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Azidomethyl-2-carboxyethylfuran → 5-Aminomethyl-2-carboxyethylfuran
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Azidomethyl-2-carboxyethylfuran | HCID 18993306 | — |
| 촉매 | Nickel | HCID 935 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 5-Aminomethyl-2-carboxyethylfuran | HCID 18993174 | 98.5% |
반응 단계
Treatment of a solution in ethanol (50 mL) at ambient temperature of 5-azidomethyl-2-carboxyethylfuran (585 mg, 3.00 mmol), prepared as in step 3, with Raney nickel 2800 and 4 atmospheres of H2 for 24 hours, followed by filtration of the reaction mixture and concentration in vacuo gave 5-aminomethyl-2-carboxyethylfuran (0.50 g) as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05486525 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-6f66f430e4d846f59b020b67e134241f |
| 출처 메모 | uspto-grants-1996_01 |