Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyanuric chloride → 4,6-dichloro-2-ethoxycarbonylmethylamino-S-triazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyanuric chloride | HCID 7954 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | Glycine ethyl ester, hydrochloride | HCID 2723640 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 4,6-dichloro-2-ethoxycarbonylmethylamino-S-triazine | HCID 14746261 | — |
반응 단계
36.9 g of cyanuric chloride, 27.9 g of ethyl glycinate hydrochloride and 33.6 g of sodium bicarbonate were heated under reflux in 200 ml of dioxane for 30 minutes. At the end of this time, the dioxane was removed by distillation under reduced pressure, and a mixture of ethyl acetate and water was added to the resulting residue, after which the mixture was shaken.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05486556 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-bd7a9204833e44b8adfa2e160635c080 |
| 출처 메모 | uspto-grants-1996_01 |