돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 37602생성일: 2026년 10월 26일

4-Vinyl-1-cyclohexene → 6-(3-Hexenyl)-4,4-dichloro-4-sila-1-hexene

https://huagongshe.com/reaction/37602

반응식

참여 물질

역할이름HCID투입량
반응물4-Vinyl-1-cyclohexeneHCID 7499—
반응물Dichloro(prop-2-enyl)silaneHCID 77536—
촉매Chloroplatinic acidHCID 61859—
용매IsopropanolHCID 3776—
생성물6-(3-Hexenyl)-4,4-dichloro-4-sila-1-hexeneHCID 5708900476,753.602%

반응 단계

Using the same apparatus and procedure described in EXAMPLE 1, 37.8 g (0.35 mol) of 4-vinylcyclohexene and 60 μl of 1% chloroplatinic acid in isopropanol were added to the flask. Through the dropping funnel was added dropwise 10.0 g (0.07 mmol) of allyldichlorosilane for 30 min at 80° C. and the solution was further reacted for 3 hrs to complete the reaction. Vacuum distillation (70-73° C./0.5 torr) of the product mixture gave 13.5 g (78%) of 6-(3-hexenyl)-4,4-dichloro-4-sila-1-hexene.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05420323
출처 데이터셋uspto-grants-1995_05
ORD IDord-a6e6ebd445904251982b712987aa6c82
출처 메모uspto-grants-1995_05