Ethylamine → HCID 690464, 화합물

반응식

[Cl:1][C:2]1[CH:10]=[CH:9][C:8]([Cl:11])=[CH:7][C:3]=1[C:4](Cl)=[O:5].[CH2:12]([NH2:14])[CH3:13]>>[CH2:12]([NH:14][C:4](=[O:5])[C:3]1[CH:7]=[C:8]([Cl:11])[CH:9]=[CH:10][C:2]=1[Cl:1])[CH3:13]

참가 물질

반응물 2

HCID 6341Ethylamine

HCID 179452,5-Dichlorobenzoyl chloride

생성물 1

HCID 690464HCID 690464, 화합물수율 85%

실험 절차

2,5-Dichlorobenzoyl chloride (51 mmol) and 70% aq EtNH2 (130 mmol) were combined according to General Method E1 to afford 9.4 g of N-ethyl-2,5-dichlorobenzamide as a beige solid, an 85% yield.

출처 및 근거

ORD 기록: ord-cd694c4425fa4ca88f4285cf9297babd
출처 데이터셋: uspto-grants-2000_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: USRE036562

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