Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Alcohol → 1-(2-Bromophenyl)ethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Alcohol | HCID 244 | — |
| 반응물 | 2-Bromobenzyl alcohol | HCID 72850 | — |
| 반응물 | Tricyclohexyl [o-(1-hydroxyethyl)phenyl]tin | HCID 19359512 | — |
| 생성물 | 1-(2-Bromophenyl)ethanol | HCID 95455 | 75.1% |
반응 단계
17.2 g of o-[tri(cyclohexyl)]tin]benzylalcohol was obtained in the same manner as in the synthesis of tricyclohexyl[o-(1-hydroxyethyl)phenyl]tin of Example 1-(4), with the exception that 9.40 g of o-bromobenzylalcohol (50.2 mmol), prepared in the aforementioned example (1), instead of o-bromo-1-phenyl ethanol (yield=75.1%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06022822 |
| 출처 데이터셋 | uspto-grants-2000_02 |
| ORD ID | ord-3367da7ec83a4b569278ddffb8d8c220 |
| 출처 메모 | uspto-grants-2000_02 |