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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 376939생성일: 2026년 10월 24일

Benzenamine, 4-(1-methyl-1-phenylethyl)-N-[4-(1-methyl-1-phenylethyl)phenyl]- → Ethylenediamine

https://huagongshe.com/ko/reaction/376939

반응식

참여 물질

역할이름HCID투입량
반응물Benzenamine, 4-(1-methyl-1-phenylethyl)-N-[4-(1-methyl-1-phenylethyl)phenyl]-HCID 82343—
반응물(2R,3S,4S,5R,6R)-2-(hydroxymethyl)-6-[(E)-3-phenylprop-2-enoxy]oxane-3,4,5-triolHCID 5280656—
반응물2-HexadecylicosanamideHCID 21863063—
생성물EthylenediamineHCID 3301—
생성물Stearic AcidHCID 5281—

반응 조건

온도110 °C

반응 단계

In a stainless steel beaker were combined about 3170 grams of stearyl stearamide (KEMAMIDE S-180, Witco), about 1553 grams of a rosin ester tackifier resin available commercially as Arakawa KE-100 (glycerol ester of hydrogenated abietic (rosin) acid available from Arakawa Chemical Industries, Ltd. of Osaka Japan) and about 299 grams of Ink Yellow 869 (Milliken Chemical Company). In addition, about 10.0 grams of Uniroyal Naugard 445 anti-oxidant were added. The materials were melted together in a temperature controlled oven at about 140° C. The molten mixture was stirred and further heated in a controlled temperature heating mantle at about 110° C. To this stirred mixture was added about 1266 grams of UNIREZ 2970 (a dimer acid-based tetraamide material manufactured by Union Camp and formed by the reaction of one mole of dimer acid, two moles of ethylene diamine, and two moles of stearic acid) in several portions at a rate so as to avoid freezing the mixture. After stirring for about 1/2 hour, the yellow ink was filtered through a heated Mott apparatus (available from Mott Metallurgical) using #3 Whatman filter paper and a pressure of about 15 psi. The filtered phase change ink was poured into molds and allowed to solidify to form ink sticks.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06022909
출처 데이터셋uspto-grants-2000_02
ORD IDord-1fe69e3d1dc84ee4826be03db6e785bc
출처 메모uspto-grants-2000_02