Ammonia → N-(2,2-Dimethoxyethyl)thiourea
반응식
[NH3:1].[CH3:2][O:3][CH:4]([O:9][CH3:10])[CH2:5][N:6]=[C:7]=[S:8]>CO>[CH3:2][O:3][CH:4]([O:9][CH3:10])[CH2:5][NH:6][C:7]([NH2:1])=[S:8]참가 물질
4
실험 절차
Methanol (200 mL) was saturated with ammonia and stirred with isothiocyanatoacetaldehyde dimethyl acetal (5.0 g) for 2 h. The mixture was concentrated and the residue was chromatographed (silica gel, 5% methanol/dichloromethane) to give the title compound.
후처리
- concentrationThe mixture was concentrated
- customthe residue was chromatographed (silica gel, 5% methanol/dichloromethane)
출처 및 근거
- ORD 기록
- ord-a36e44436710468abec7fc2fdab510d1
- 출처 데이터셋
- uspto-grants-2000_02
- 특허 번호
- US06028087
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