Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorodimethylphenylsilane → n,n-Diethyl-2-chloro-6-(dimethylphenylsilyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorodimethylphenylsilane | HCID 13029 | — |
| 반응물 | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| 생성물 | n,n-Diethyl-2-chloro-6-(dimethylphenylsilyl)benzamide | HCID 54348567 | — |
반응 단계
The title compound was prepared from the compound of Example e and 1.1 eq dimethylphenylsilyl chloride according to General Method A. Purification by HPLC with 1:9 ethyl acetate/hexanes gave 6.3 g of the desired product as a clear oil, a 91% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06028101 |
| 출처 데이터셋 | uspto-grants-2000_02 |
| ORD ID | ord-e0368283ae8643caa50546b0ac78faf2 |
| 출처 메모 | uspto-grants-2000_02 |