Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 2-Chloro-n-hydroxy-n-(1-methylethyl)-6-(trimethylsilyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | N-Isopropylhydroxylamine Hydrochloride | HCID 170873 | — |
| 반응물 | 2-Chloro-6-(trimethylsilyl)benzoyl chloride | HCID 15183557 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 2-Chloro-n-hydroxy-n-(1-methylethyl)-6-(trimethylsilyl)benzamide | HCID 18630150 | — |
반응 단계
The title compound was prepared by reaction of the compound of Example b and the i-propylhydroxylamine hydrochloride in dioxane in the presence of two equivalents of triethylamine using the amination methods described above. m.p. 175-179° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06028101 |
| 출처 데이터셋 | uspto-grants-2000_02 |
| ORD ID | ord-f3b2352a9149482ca3a362993dc3a72a |
| 출처 메모 | uspto-grants-2000_02 |