Sodium Sulfite → (4-Cyanophenyl)methanesulfonyl chloride
반응식
Br[CH2:2][C:3]1[CH:10]=[CH:9][C:6]([C:7]#[N:8])=[CH:5][CH:4]=1.[S:11]([O-:14])([O-])=[O:12].[Na+].[Na+].P(Cl)(Cl)(Cl)(Cl)[Cl:18]>>[C:7]([C:6]1[CH:9]=[CH:10][C:3]([CH2:2][S:11]([Cl:18])(=[O:14])=[O:12])=[CH:4][CH:5]=1)#[N:8]참가 물질
4
실험 절차
4-Bromomethylbenzonitrile was reacted with sodium sulphite followed by phosphorus pentachloride to give 4-cyanobenzylsulphonyl chloride which was reacted with pentylamine in a similar manner to N14 to give the title compound.
출처 및 근거
- ORD 기록
- ord-c5820895b0e64197a7070d5335e7b0e1
- 출처 데이터셋
- uspto-grants-2000_02
- 특허 번호
- US06031109
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