참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phenol | HCID 996 | — |
| 반응물 | 4,5-Dihydro-2,4,4-trimethyloxazole | HCID 74496 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | N-(1,1-dimethyl-2-phenoxyethyl)acetamide | HCID 18349669 | — |
반응 단계
A mixture of phenol (33.2 g) and 2,4,4-trimethyloxazoline (18.1 g) was heated in a stirred pressure vessel at 220° C. for 48 hours. The oil obtained on cooling was dissolved in ethyl acetate, washed with 5M sodium hydroxide solution, water, brine, then dried and evaporated to give an oil which was distilled under high vacuum to give N-(1,1-dimethyl-2-phenoxyethyl)acetamide, b.p. 115-122° C. at 0.67 mbar.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06031109 |
|---|
| 출처 데이터셋 | uspto-grants-2000_02 |
|---|
| ORD ID | ord-74f7b1681da446ec8ea0f484ba7dcf7f |
|---|
| 출처 메모 | uspto-grants-2000_02 |
|---|
