Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → (2,6-Dichlorophenyl)methanesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | (2,6-Dichlorophenyl)methanesulfonyl chloride | HCID 594465 | — |
| 생성물 | (2,6-Dichlorophenyl)methanesulfonamide | HCID 13631936 | 64% |
반응 단계
The 2,6-dichlorobenzylsulfonylchloride (27 g, 103.6 mmol) in ammonium hydroxide (270 ml) was stirred at room temperature for about 3 hours. On acidification with cooled concentrated hydrochloric acid a precipitate separated and was filtered to give desired product (16 g, 64%) EI-MS m/z 239 (M−).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06297265B2 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-796a401721d446ecaafb9db34d1d068f |
| 출처 메모 | uspto-grants-2001_10 |