Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → Methyl [(4-nitro-phenyl)-phenyl-amino]-acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-Nitrodiphenylamine | HCID 13271 | — |
| 반응물 | Methyl bromoacetate | HCID 60984 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Methyl [(4-nitro-phenyl)-phenyl-amino]-acetate | HCID 54362794 | — |
반응 단계
4-Nitro-diphenylamine (Aldrich) is reacted with methyl bromoacetate in the presence of potassium carbonate in DMF at 70° C. to give methyl [(4-nitro-phenyl)-phenyl-amino]-acetate (brown oil). MS: 287 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06297266B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-4befb3919eea43d0a93eef70b3a9de60 |
| 출처 메모 | uspto-grants-2001_10 |