Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methylbenzyl alcohol → 2-Methylbenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methylbenzyl alcohol | HCID 6994 | — |
| 반응물 | O-Xylene | HCID 7237 | — |
| 반응물 | 3-amino-N-hydroxyphthalimide | HCID 10888472 | — |
| 생성물 | 2-Methylbenzaldehyde | HCID 10722 | 30% |
반응 단계
170 mg (1.60 mmol) of o-xylene were reacted analogously to Example 1 in the presence of 32.1 mg (0.180 mmol) of 3-amino-N-hydroxyphthalimide. After a reaction time of 4 hours and 18 hours, a further 32.1 mg (0.180 mmol) of 3-amino-N-hydroxyphthalimide were added in each case, and, after a total of 30 hours, the reaction solution was extracted with chloroform and examined by NMR spectroscopy. Yield 30% of 2-methylbenzaldehyde and 7% of 2-methylbenzyl alcohol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06297403B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-1891e06b840d49d48dfd203a556d703d |
| 출처 메모 | uspto-grants-2001_10 |