Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrate lead acetate → Lead diacetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrate lead acetate | HCID 86584228 | — |
| 용매 | 2-Butoxyethanol | HCID 8133 | — |
| 생성물 | Lead diacetate | HCID 9317 | — |
반응 단계
The hydrate lead acetate is dissolved in butoxyethanol (BuEtOH) (1) at 60° C. The resulting solution is kept at this temperature for two hours, and is cooled down slowly (2) to thereby form a precipitate of dehydrated lead acetate. The precipitation yield can be promoted by further cooling down the vessel containing said solution in an ice bath.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06300144B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-d2912ed95edd4b108b23c3a7feb1bdf4 |
| 출처 메모 | uspto-grants-2001_10 |