Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl[2-(4-nitrophenoxy)ethyl]amine → 4-(2-(Diethylamino)ethoxy)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl[2-(4-nitrophenoxy)ethyl]amine | HCID 88294 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-(2-(Diethylamino)ethoxy)aniline | HCID 418932 | 98.4% |
반응 단계
N,N-diethyl-2-(4-nitrophenoxy)ethylamine (28.19 g) was dissolved into methanol (300 ml) and subjected to hydration reaction at ambient pressure by adding 10% palladium carbon catalyst (1.5 g). After completion of hydration reaction, catalyst was removed by filtration. Filtrate was concentrated under vacuum to obtain N,N-diethyl-2-(4-aminophenoxy)ethylamine (24.25 g) as color-less oily substance.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06300368B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-72a8bec4006c486aac01b693cc55603e |
| 출처 메모 | uspto-grants-2001_10 |