2-Bromo-1-(3-methylphenyl)ethan-1-one → HCID 18368201, 화합물

HRID 379788

반응식

HRID 379788 반응식
[CH2:1]([O:3][C:4]([NH:6][C:7]1[CH:14]=[CH:13][C:12]([N+:15]([O-:17])=[O:16])=[CH:11][C:8]=1[C:9]#[N:10])=[O:5])[CH3:2].Br[CH2:19][C:20]([C:22]1[CH:27]=[CH:26][CH:25]=[C:24]([CH3:28])[CH:23]=1)=[O:21]>C(OCC)(=O)C>[NH2:10][C:9]1[C:8]2[C:7](=[CH:14][CH:13]=[C:12]([N+:15]([O-:17])=[O:16])[CH:11]=2)[N:6]([C:4]([O:3][CH2:1][CH3:2])=[O:5])[C:19]=1[C:20](=[O:21])[C:22]1[CH:27]=[CH:26][CH:25]=[C:24]([CH3:28])[CH:23]=1

참가 물질

4

반응물 2

HCID 100361292-Bromo-1-(3-methylphenyl)ethan-1-oneHCID 183679462-(Ethoxycarbonylamino)-5-nitrobenzonitrile

생성물 1

HCID 18368201HCID 18368201, 화합물

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

The title compound was prepared according to the procedure described in step 2 of Example 1 from 2-(ethoxycarbonylarnino)-5-nitrobenzonitrile (Example 96, step 1) and 2-bromo-3′-methylacetophenone. tlc: Rf=0.6 (33% ethyl acetate in hexanes)

출처 및 근거

ORD 기록
ord-00f8cf3fc0d64fb380f68bfd594307d8
출처 데이터셋
uspto-grants-2001_10
특허 번호
US06300363B1

연결된 노트

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