Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Chloride → HCID 178418536, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Chloride | HCID 6327 | — |
| 반응물 | 4-Chlorophenyl Isocyanate | HCID 7693 | — |
| 반응물 | 3-[4-(4-Chlorobenzyl)piperazin-1-yl]propanethiol dihydrochloride | HCID 13731118 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | HCID 178418536 | HCID 178418536 | 42.4% |
반응 단계
The procedure described in Example 2 was followed, using 1.5 g of 4-chlorophenyl isocyanate, 3.5 g of 3-[4-(4-chlorobenzyl)piperazin-1-yl]propanethiol dihydrochloride, 1.2 g of triethylamine and 50 ml of methyl chloride, to give 1.1 g (21% of theory) of N-(4-chlorophenyl)-S-{3-[4-(4-chlorobenzyl)piperazin-1-yl]propyl}thiocarbamate dihydrochloride monohydrate as an off-white crystalline solid, M.p. 243°-245° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04722926 |
| 출처 데이터셋 | uspto-grants-1988_02 |
| ORD ID | ord-d33367d8f1b54a0ba584c0599674b958 |
| 출처 메모 | uspto-grants-1988_02 |