Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → 1,3,5-Adamantanetriol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 1-Adamantanol | HCID 64152 | — |
| 반응물 | 1,3-Adamantanediol | HCID 573829 | — |
| 생성물 | 1,3,5-Adamantanetriol | HCID 9899022 | — |
반응 단계
One mol of 1,3-dihydroxyadamantane was stirred in an acetic acid-acetic anhydride solution of CrO3, oxidizing agent, with heating. After carrying out the reaction for 8 hours, the reaction solution was neutralized to obtain a mixture of polyhydroxylated compounds of hydroxyadamantane. This mixture was partitioned by high performance liquid chromatography to obtain 1,3,5-trihydroxyadamantane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06303266B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-ff369154e4064238a3a09741c5fa9017 |
| 출처 메모 | uspto-grants-2001_10 |