Methyl 4-methylaminobenzoate → HCID 20640608, 화합물

HRID 380365

반응식

HRID 380365 반응식
COCOC1C=C([C@@H](N2CC[C@H](OCOC)C2)CO)C=CC=1.[CH3:23][O:24][CH2:25][O:26][C:27]1[CH:28]=[C:29]([C@H:33](O)[CH2:34][N:35]2[CH2:39][CH2:38][C@H:37]([O:40][CH2:41][O:42][CH3:43])[CH2:36]2)[CH:30]=[CH:31][CH:32]=1.[CH3:45][NH:46][C:47]1[CH:56]=[CH:55][C:50]([C:51]([O:53][CH3:54])=[O:52])=[CH:49][CH:48]=1>>[CH3:23][O:24][CH2:25][O:26][C:27]1[CH:28]=[C:29]([C@H:33]([N:46]([C:47]2[CH:56]=[CH:55][C:50]([C:51]([O:53][CH3:54])=[O:52])=[CH:49][CH:48]=2)[CH3:45])[CH2:34][N:35]2[CH2:39][CH2:38][C@H:37]([O:40][CH2:41][O:42][CH3:43])[CH2:36]2)[CH:30]=[CH:31][CH:32]=1

참가 물질

4

반응물 3

HCID 140375Methyl 4-methylaminobenzoateHCID 20640583HCID 20640583, 화합물HCID 206405872-(R)-(3-methoxymethoxyphenyl)-2-(3-(S)-methoxymethoxypyrrolidin-1-yl)ethanol

생성물 1

HCID 20640608HCID 20640608, 화합물수율 60%

실험 절차

This was prepared from the mixture of 2-(R)-(3-methoxymethoxyphenyl)-2-(3-(S)-methoxymethoxypyrrolidin-1-yl)ethanol and 1-(S)-(3-methoxymethoxyphenyl)-2-(3-(S)-methoxymethoxypyrrolidin-1-yl)ethanol and methyl 4-methylaminobenzoate in 60% yield according to a procedure similar to that described in Example 1 (i).

출처 및 근거

ORD 기록
ord-fec011fe87b6452c8acf7cc3a48dac39
출처 데이터셋
uspto-grants-2001_10
특허 번호
US06303602B1

연결된 노트

불러오는 중…