Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-6-chlorobenzoic acid → HCID 20670057, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-6-chlorobenzoic acid | HCID 75071 | — |
| 반응물 | 2-(Adamantan-1-yl)ethan-1-amine hydrochloride | HCID 2771138 | — |
| 생성물 | HCID 20670057 | HCID 20670057 | — |
반응 단계
Prepared according to the method of Example 14 from 1-adamantaneethylamine hydrochloride (CN 26482-53-1) (0.105 g) and 2-amino-6-chlorobenzoic acid (0.132 g) and purified by supercritical fluid chromatography eluting with CO2 in ethanol to give the title compound, contaminated with 0.35 mol equivalents of imidazole, as a white solid (0.046 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06303659B2 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-51bde03cf1b741c4b567555a9bcc58a0 |
| 출처 메모 | uspto-grants-2001_10 |