Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Chloro-2,4-Dinitrobenzene → 2-(2,4-Dinitrophenoxy)ethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Chloro-2,4-Dinitrobenzene | HCID 6 | — |
| 반응물 | Ethylene Glycol | HCID 174 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | 2-(2,4-Dinitrophenoxy)ethanol | HCID 76070 | 74.5% |
반응 단계
20.25 g (0.1 mole) of 2,4-dinitrochlorobenzene, 124 g (2 moles) of ethylene glycol, 82.93 g (0.6 mole) of potassium carbonate, and 600 ml of xylene were placed in a reaction vessel to be stirred by heating for 12 hours. The reacted solution was isolated by filtration, and the filtrate was concentrated. 17.0 g of 2-(2,4-dinitrophenoxy) ethanol was yielded by column purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06303742B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-62be93d1b7c1453a9a1721b3f0fd489f |
| 출처 메모 | uspto-grants-2001_10 |