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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 380727생성일: 2026년 10월 25일

2-(Chloromethyl)-3,5-dimethyl-4-nitropyridine → HCID 178488124, 화합물

https://huagongshe.com/reaction/380727

반응식

참여 물질

역할이름HCID투입량
반응물2-(Chloromethyl)-3,5-dimethyl-4-nitropyridineHCID 11217896—
반응물HCID 178488032HCID 178488032—
생성물HCID 178488124HCID 178488124—

반응 단계

The 2-chloromethyl-3,5-dimethyl-4-nitropyridine of formula-III is dissolved in a protic solvent and reacted with 2-mercapto-5-methoxy benzimidazole of the formula-VII with a base to get 5-methoxy-2-(((3,5-dimethyl-4-nitro-2-pyridinyl)methyl)thio)-1H-benzimidazole of formula-VIII. After recrystallization from suitable solvents, pure compound-VIII is obtained with an impurity, 5-methoxy-2-(((3,5-dimethyl-4-chloro-2-pyridinyl)methyl)thio-1H-benzimidazole, of formula-XV less than 0.1%.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06303787B1
출처 데이터셋uspto-grants-2001_10
ORD IDord-56fb476b47e94dd8b934d9f4817f7c64
출처 메모uspto-grants-2001_10