Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Tetralone → 1,2-Dihydro-4-methylnaphthalene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Tetralone | HCID 10724 | — |
| 반응물 | HCID 178418373 | HCID 178418373 | — |
| 생성물 | 1,2-Dihydro-4-methylnaphthalene | HCID 582327 | 68% |
반응 단계
α-Tetralone was reacted with methylmagnesium iodide as described in J. Org. Chem., 26, 4165 (1961), without isolation of the intermediate 1-methyl-1-tetralol, to give the desired product, after distillation, in 68% yield as a colorless oil, boiling point 55-57° C. at 0.8 mm Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06307085B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-f467ee58ecf64abf885a0a6430418e94 |
| 출처 메모 | uspto-grants-2001_10 |