Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → HCID 178418563, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 1-Isocyanato-4-methoxybenzene | HCID 79443 | — |
| 반응물 | 3-[4-(4-Chlorophenethyl)piperazin-1-yl]propanethiol dihydrochloride | HCID 13731126 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178418563 | HCID 178418563 | 49.8% |
반응 단계
The procedure described in Example 2 was followed, using 1.7 g of 4-methoxyphenyl isocyanate, 4.0 g of 3-[4-(4-chlorophenethyl)piperazin-1-yl]propanethiol dihydrochloride, 1.1 g of triethylamine and 50 ml of methylene chloride, to give 1.4 g (25% of theory) of N-(4-methoxyphenyl)-S-{3-[4-(4-chlorophenethyl)piperazin-1-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, M.p. 236°-238° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04722926 |
| 출처 데이터셋 | uspto-grants-1988_02 |
| ORD ID | ord-524f4e4c964d4f9a84b265af1db184ef |
| 출처 메모 | uspto-grants-1988_02 |