Cinnamoyl Chloride → (E)-5-Nitro-1-(2-pyridyl)-2-styryl-1H-benzimidazole

HRID 382557

반응식

HRID 382557 반응식
[NH2:1][C:2]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[CH:11][C:3]=1[NH:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][N:6]=1.[C:18](Cl)(=O)/[CH:19]=[CH:20]/[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1.N1C=CC=CC=1N1C2C=CC=CC=2N=C1/C=C/C1C=CC=CC=1>>[N+:15]([C:13]1[CH:12]=[CH:11][C:3]2[N:4]([C:5]3[CH:10]=[CH:9][CH:8]=[CH:7][N:6]=3)[C:18](/[CH:19]=[CH:20]/[C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)=[N:1][C:2]=2[CH:14]=1)([O-:17])=[O:16]

참가 물질

4

반응물 3

HCID 5354261Cinnamoyl ChlorideHCID 9796241(E)-1-(2-pyridyl)-2-styryl-1H-benzimidazoleHCID 12672123HCID 12672123, 화합물

생성물 1

HCID 22736675(E)-5-Nitro-1-(2-pyridyl)-2-styryl-1H-benzimidazole

실험 절차

The titled compound was prepared from 2-(2-amino-4-nitroanilino)pyridine (Runti, C. Ann. Chim. (Rome), 1956, 46, 406) and (E)-cinnamoyl chloride according to the preparation of (E)-1-(2-pyridyl)-2-styryl-1H-benzimidazole (Example 1, method A).

출처 및 근거

ORD 기록
ord-56f8e8a466004587ad5198b60bce404d
출처 데이터셋
uspto-grants-2001_10
특허 번호
US06310079B1

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