Diethanolamine → 5-Amino-3-acetoxymethyl-N,N-bis(2-hydroxyethyl)-2,4,6-triiodobenzamide

HRID 383041

반응식

HRID 383041 반응식
[NH2:1][C:2]1[C:3]([I:18])=[C:4]([CH2:13][O:14][C:15](=[O:17])[CH3:16])[C:5]([I:12])=[C:6]([C:10]=1[I:11])[C:7](Cl)=[O:8].[NH:19]([CH2:23][CH2:24][OH:25])[CH2:20][CH2:21][OH:22]>>[NH2:1][C:2]1[C:3]([I:18])=[C:4]([CH2:13][O:14][C:15](=[O:17])[CH3:16])[C:5]([I:12])=[C:6]([C:10]=1[I:11])[C:7]([N:19]([CH2:23][CH2:24][OH:25])[CH2:20][CH2:21][OH:22])=[O:8]

참가 물질

3

반응물 2

HCID 8113DiethanolamineHCID 184293385-Amino-3-acetoxymethyl-2,4,6-triiodobenzoyl chloride

생성물 1

HCID 184292425-Amino-3-acetoxymethyl-N,N-bis(2-hydroxyethyl)-2,4,6-triiodobenzamide

실험 절차

5-Amino-3-acetoxymethyl-2,4,6-triiodobenzoyl chloride was reacted with diethanolamine according to the general procedure in Example 24g. Yield of isolated crude product was 98%.

후처리

  1. customYield of isolated crude product

출처 및 근거

ORD 기록
ord-42d32b5b1760434bbe916edbdda2234b
출처 데이터셋
uspto-grants-2001_10
특허 번호
US06310243B1

연결된 노트

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