Ethanolamine → 5-Amino-3-acetoxymethyl-N-(2-hydroxyethyl)-2,4,6-triiodobenzamide

HRID 383044노트

반응식

HRID 383044 반응식
[NH2:1][C:2]1[C:3]([I:18])=[C:4]([CH2:13][O:14][C:15](=[O:17])[CH3:16])[C:5]([I:12])=[C:6]([C:10]=1[I:11])[C:7](Cl)=[O:8].[CH2:19]([CH2:21][NH2:22])[OH:20]>>[NH2:1][C:2]1[C:3]([I:18])=[C:4]([CH2:13][O:14][C:15](=[O:17])[CH3:16])[C:5]([I:12])=[C:6]([C:10]=1[I:11])[C:7]([NH:22][CH2:21][CH2:19][OH:20])=[O:8]

참가 물질

3

반응물 2

HCID 700EthanolamineHCID 184293385-Amino-3-acetoxymethyl-2,4,6-triiodobenzoyl chloride

생성물 1

HCID 184292535-Amino-3-acetoxymethyl-N-(2-hydroxyethyl)-2,4,6-triiodobenzamide

실험 절차

5-Amino-3-acetoxymethyl-2,4,6-triiodobenzoyl chloride was reacted with ethanolamine according to the general procedure in Example 24 g. The yield of isolated product was 98%.

출처 및 근거

ORD 기록
ord-0cfb6b09b14f46bb861e083000f8d71c
출처 데이터셋
uspto-grants-2001_10
특허 번호
US06310243B1

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